摘要: |
目的:建立骨刺胶囊的质量标准。方法:采用显微鉴别法鉴别全蝎、土鳖虫、白芍;采用薄层色谱法(TLC)鉴别白芍、延胡索、威灵仙、龙血竭。结果:显微鉴别特征明显;薄层色谱相应主斑点清晰,分离度好,且阴性无干扰。结论:本文建立的方法专属性强、重复性好,可用于骨刺胶囊的质量控制。 |
关键词: 骨刺胶囊 质量标准 显微鉴别 薄层色谱 |
DOI: |
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A study of the quality standard for Guci capsules |
TANG Chang-li,,LIU Ting,,TIAN Qi-xue |
(The People’s Hospital of Mayang Miao Autonomous County,Mayang 419400,Hunan,China;The hospital of Hunan Traditional Chinese Medicine Academy,Changsha 410006,Hunan,China) |
Abstract: |
Objective:To establish the quality standard for Guci capsules.Methods:Microscopic identification was used to identify scorpion,Eupolyphaga steleophaga,and Radix Paeoniae Alba;thin-layer chromatography(TLC)was used for the identification of Radix Paeoniae Alba,Rhizoma Corydalis,Clematis chinensis,and Resina Draconis.Results:Microscopic identification had marked features.There were clear and well separated TLC spots,with no interference from negative control.Conclusion:The method established in this study has good specificity and repeatability and can be used for the quality control of Guci capsules. |
Key words: Guci capsule quality standard microscopic identification thin-layer chromatography |